If your data are organized as in 3 columns. First column X, 2nd Y and 3rd Z, Please set the 3rd column as Z and then choose Worksheet: Convert to Matrix: XYZ Gridding... to convert it into matrix.
Actually Origin supports plotting 3D data directly from XYZ columns in worksheet. So you can highlight the Z column (must be set as Z) and then plot: 3D Surface: and pick the plot type you want.