Hi, OriginLab forum,
I'm doing some data analysis for a previous researcher whose data came out pretty messy. Still, it has some interesting characteristics that I'm trying to clean up so I can glean some more information. There are three 2(theta) x-values that I need to integrate for several thousand frames of collected data. Since the data set is so enormous I am trying to take advantage of the "batch peak analyzer". I've done some initial clean-up and integrations, but I've noticed some spots where peaks start to split or are not present. I'm a bit concerned about whether this trend is not accounted for when I am running the integrations. How would you fellow XRD analyzers do this kind of analysis? Ultimately I am looking to calculate the lattice parameters as a function of time.
I've also been running into an error saying that the data is locked when I try to run another peak analyzer batch for the second/third 2(theta). None of my columns are truly locked and I can't find what this is referring to. Any direction about that would be great!
Origin Ver. and Service Release (Select Help-->About Origin): OriginPro 2024 (64-bit) (Academic)
Operating System: Windows 10 and Windows 11 |
Messy XRD -- Peak fitting
Posted - 07/19/2024 : 6:56:56 PM
